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极谱痕量分析仪 (433-A型)

主要特点

  • 金属痕量分析精度达1µg/L水平
  • 有机物分析
  • 理想用于质量和过程控制实验室
  • 用于多种研究工作

痕量分析从来没有像今天这样如此受重视!饮水、食品、饮料等样品中的重金属和其它污染物需要连续的监测。极谱痕量分析仪是一套独立的紧凑系统,由高精度的静汞滴电极和完全计算机化的痕量分析仪结合组成,应用于全新的极谱法和伏安法相结合的领域。

 

一套完整的433-A型极谱痕量分析仪不需要外部附件就可以投入工作:只需要连接到任何一台个人电脑上就可以进行分析了。

基于Windows©操作系统的软件随仪器配送。

 

汞泵——仪器的心脏

433-A型极谱痕量分析仪的绝大多数性能都依赖于独一无二设计的汞分配装置和毛细管。

在相似的其它仪器中曾经出现过的问题在此处完全被摒除了:没有压制、没有直接与汞接触的结构,完美的汞滴重现性,简单易于替换的毛细管延长了工作寿命而又不改变仪器的精度。

 

完全装配的电解池头

 

The supporting block contains a complete set of electrodes, two-way gas purging inlet/outlet, sample injection port and full sealing to insure a complete tightness of the cell (available in different materials and shapes).

 

A rotating-field magnetic stirrer provides accurate solution stirring during sample purging or anodic stripping. All parts in contact with the solution are made in Teflon®, Viton® or Silicone Rubber® for long life and minimum pollution of samples. The built-in electrodes can be easily removed for cleaning, refilling or to be replaced with external ones: for this purpose a set of connections is made available on the cell block itself

No longer mercury free on the lab!

The mercury reservoir is another unique AMEL innovation: made completely out of polypropilene, it is fully sealed with respect the outside ambient allowing safe operation under any condition without risks for ambient pollution. A plastic rotating cock allows complete isolation of the reservoir from the valve in order to replace the latter without empty the former. The large reservoir capacity (about 3 kg) allows months of continuous operation without refilling need; the tightness of the reservoir preserves the mercury from pollution and dust. The 433 can be moved around in the lab or even transported by car for short distances filled up without spillage risk!

 
The application software

Application software allows to perform almost all presently known polarographic and voltammetric techniques including SQUARE WAVE, STRIPPING ANALYSIS, CYCLIC VOLTAMMETRY, etc.

This package runs under WINDOWS® and requires at least a 486 PC fitted with a colour VGA monitor, 8 Mbytes of RAM MEMORY, 66 Mhz clock frequency, serial and a parallel port, a mouse and 3.x WINDOWS ® (or WINDOWS 95 ®) operating system.

This program allows to perform trace polarographic, voltammetric and stripping analysis with the greatest ease interfacing the instrument with a clear-menu driven sequence, options, graphic manipulations and file management using all features and advantages of windows operating system. The above program is supplied on a single HD 3,5 diskette and must be installed on the computer's Hard disk for execution and use.

Download Software DEMO for Windows 3.x and 95 (600Kb)

 
Available Techniques supplied software
POLAROGRAPHY
VOLTAMMETRY
ANODIC STRIPPING
*.D.C. *.D.C. *.D.C.
*TAST *Cyclic  
*Normal Pulse *Differential Pulse *Differential Pulse
*Differential Pulse *Square Wave *Square Wave
  *Staircase
 
Fields of Application
In the following table we list the most important classes of ORGANIC COMPOUNDS which can be subjected to VOLTAMMETRIC or POLAROGRAPHIC analysis
ACIDS
Ascorbic, Fumaric, Maleic, Salicilic, Oxalic, Phtalic, NTA, EDTA, Lactic, Acetylsalycilic, Tartaric, Boric
ALDHEYDES
Formaldheyde,Benzoic, Citral
KETONES
Anthraquinone, Acetone
AROMATICS
Antioxidisers, Nitrobenzoic Acid, Butyl-cathecol and p-metoxiphenol, Chloroamphenicol, Phenylbutazone, Oxiphenbutazone
HALOGEN DERIVATES
DDT, Pesticides
ALCOHOLS
Diols, Quinhydrone
AMMINES
Hydrazine, Ammonia, Aniline, Pyridine
AMIDES
Thiourea, Phtalimide
SUGARS
Fructose
MISCELLANEOUS
Saccharine, Vanillin, Nicotine, Metylen-bisthiocyanate, Tetracycline, Liposoluble, Vitamins, Amino-acids, Theophylline, Veronal, Quinine, Bilirubin...

 

The principal application areas are listed:
FOODS
  • DRINKS: Lead, Cadmium, Chromium, Cobalt, Fructose, Saccaharine
  • FRUIT JUICES: Vitamin C, Lead, Cadmium, Preservatives
  • WINES: Lead, Cadmium, Copper, Sulphites, Fructose, Aminoacids
  • OILS: Vitamins, Nickel, Antioxidisers, SO2MEAT: Lead, Nickel, Nitrates, Nitrites, ZincFRUITS: Vitamin C, Organic acidsCEREALS: Lead, Cadmium, Chromium, Copper, IronMILK: Cadmium
WATERS
  • Lead, Cadmium, Chromium, Cobalt, Copper, Nickel, Zinc, Tin, Molybdenum, Boric Acid, Saccharine, Formaldehyde, Cyanides, Bismuth, Antimony, Vanadium, Titanium, Manganese
MINERAL SOILS
and METALLURGY
  • All Metals
COSMETICS
and DETERGENTS
  • Preservatives, Lead, Cadmium, Formaldehyde, Arsenic, EDTA, NTA
PHARMACEUTICALS
  • Active principles, even in complex matrices. Chloroamphenicol, Tetracycline, Vitamins, Amino-acids, Theophylline, Veronal
BIOLOGY
  • Heavy metals in human blood and other biological fluids (urine)
MEDICINE
  • Bilirubin, Morphine

 
Technical Specifications
Potentiostat
  • Output Voltage Compliance: ±12V
  • Output Current: ±10mA
  • Response Time: ±10µS
i/E Converter
  • Current Scales: Six decades ±20nA, ±2mA
  • Output Signal at full scale: ±10V
  • Response Time: ±10µS
  • Filter Time Constant: 600mS
Analog to Digital Converter
  • Type: Successive Approximation
  • Resolution:12bits, bipolar
  • Conversion Time: 25µS typical
Digital to AnalogConverter
  • Resolution:16bits, bipolar
  • Linearity: ±0.003% of full scale
  • Settling Time: 3µS typical
  • Output Signal: ±4.095V or ±2.047V
Backing-off Converter
  • Compensation Range: ±200% of full scale
  • Resolution:8bits, bipolar
Electrodes
  • Capillary: Glass 135x6 mm. Bore 0.1 mm
  • Counter Electrode: Platinum Wire 5x1 mm
  • Reference: Ag-AgCI Filled with saturated KCl
Digital Interface
  • Type: Serial standard RS-232C FULLY OPTO-INSULATED
  • Lines: TX, RX, GND, RTS, CTS, DCD, DTR
  • Baud Rates: 600, 1200, 2400, 4800, 9600
Digital Section
  • Microprocessor: Z80-A CPU (4MHz)
  • Program Memory: C-MOS RAM 32Kx8 with backup battery (six months retention)
  • Local Console: LCD alphanumeric display with two rows of 16 characters
Setup Parameters
  • Potential Ranges: ±2.047V or ±4.095V with 62.58µV or 125µV resolution
  • Scan Increment: 62.5µV minimum
  • Scan Rates: from 1µV/s up to about 300mV/s higher rates degrade resolution
  • Pulse Height: ±2V with 62.5µV resolution
  • Pulse Duration: up to 65s with 1ms increment
  • Drop Size: 80 different sizes
  • Drop Time: 1 to 10 seconds
  • Purge Time: 0 to 30 minutes
  • Stirring Time: 0 to 30 minutes
  • Stirring Speed: 100 to 800 r.p.m.
  • Replications: 1 to 256
  • Data Points: up to 6140 couples current-potential can be stored consecutivele
Power Supply
  • 110/220V a.c.: 40-60Hz: 60VA max
Size and Weight
  • Size: 200x300 mm; 390 mm height;
  • Weigth: 10 kg without mercury and accessories
 
       
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